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铝合金表面氧化锆等离子体电解氧化涂层的制备及形成机理研究

辛世刚,赵荣根,都徽,宋力昕

无机材料学报 doi:10.3724/SP.J.1077.2009.00107

采用等离子体电解氧化方法在铝合金表面制备了氧化锆涂层,电解液为包含Zr(OH)4颗粒的碱性溶液. 涂层的组成、结构通过XRD、EPMA进行了研究. 结果显示,涂层主要由t-ZrO2、m-ZrO2α-Al2O3和γ-Al2O3组成,t-ZrO2为涂层的主晶相,分布在涂层表面,而α-Al2O3出现在涂层的内侧.涂层表面呈颗粒状,颗粒尺寸约为1~2μm.在氧化过程中,Zr(OH)4颗粒在电场力的作用下向等离子体放电通道口沉积,在放电产生的高温作用下直接转化为氧化锆.

关键词: 氧化锆 , coating , plasma electrolytic oxidation , aluminium alloy

Al-Si合金等离子涂层Ni-Cr-B-Si的激光重熔

梁工英 , 李成劳 , 苏俊义

金属学报

利用5kWCO2激光器重熔Al-Si合金表面的Ni-Cr-B-Si等离子喷涂层.SEM和TEM分析结果表明,激光熔层内晶化区和非晶化区共存,在后续熔区的传热作用和周围结晶潜热作用下,有部分非晶晶化为Ni3Al纳米晶(2—5nm),其中一些逐渐长大成为细小的粒状晶.未晶化区硬度极高(HV=1235),是原等离子喷涂层硬度的4倍。

关键词: 激光表面熔化 , aluminium alloy , amorphous , nanocrystal

BACKGROUND RECTIFICATION AND FEATURE EXTRACTION OF IMAGE IN A SPOT WELD OF AL ALLOY X-RAY DETECTION

T.Gang , J.Zhang , M.B.Zhang and F.X.Liu (1)AWPT National Key. , HIT , Harbin 15001 , China 2)State 159 Factory , China)

金属学报(英文版)

A primary study on Processing in X - ray inspection of spot weld for aluminum alloy spot welding,in- cluding for background simulation,acquisition of ideal binary image, and extraction and identifi- cation of defect features was presented.

关键词: X - ray detection , null , null , null

SIMULATION PROCESS IN LASER WELDING Ⅱ

Y. P. Kathuria (Laser X Co. Ltd. Chick - shi Aichi - ken 472 , Japan)

金属学报(英文版)

With the established technique of laser in science and industry, its applications hare become diversified in the automotive welding.Two potential lasers CO2 and Nd - YAG operating in the i. r. region hare been applied in various demains covering different spectrum of welding,ranging from dissimilar matal to aluminium alloy welding.These lasers considered as thermal processing tools offers an advantage of the keyhole welding offered by the electron beam where the energy is transferred from the surface by the keyhole formation. with the incorporation of these lasers as a flexible thermal processing tool,it has become essential to use them optimally through feedback with planning and constructional rules.Based upon the modulation and duty cycle variation,a simulation technique is demonstrated which enable us to estimate the processing results and determine the characterisitcs of the fabricated part. From the giv- en provess parameters such as haer power, focus radius,processing speed /interaction time and materi- al characteristics, one can optimize the welding condition etc. through the simulation process. In the present work the laser simulation process in welding were carried out with Al- alloy A 5052 of various thickness by using a multiwave high power Nd - YAC lasers.The simulated weld conditions resulted in better utility of the lasers with increased efficiency and better quality. The use of simuation method helped in the designing and prediction of welding technology, which reduced the rejection rate as well as the cost of production.

关键词: easer beam welding , null , null , null

STUDY OF K_(2)O·6TiO_(2) WHISKER REINFORCED AI COMPOSITES FOR THEIR MECHANICAL PROPERTIES AND INTERFACIAL STRUCTURES

PA N JinChangsha Institute of Technology , ChinaLI Jihong , NING Xiaoguang , YE HengqiangLab. of Atomic Imaging of Solids , Institute of Metal Research , Chinese Academy of Sciences. Shenyang , China Manuscript received 28 February , 1994

金属学报(英文版)

A newly developed whisker K_(2)O 6TiO_(2) reinforced 6061 Al composite was prepared by squeeze casting process. The flexural strength of the composite is 518MPa, and decreases to 490 M Pa after T6 treatment.The hardness of the composite also shows the similar change while T6 treating. The results of HRTEMobservation may explaine this property change. It was considered that there is a continuous TiO layer at the whisker-matrix interface, which is easily to react with the segregated Mg and to form MgTi_(2)O_(4), MgAl_(2)O_(4). The thickening of TiO layer after T6 treatment is the main reason resulting in strength degradation of composite.

关键词: potassium titanate. whisker , null , null

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